Information card for entry 7156739

Structure parameters

• Formula: C26 H49 N O4 Si2
• Calculated formula: C26 H49 N O4 Si2
• Title of publication: Total synthesis of spiromastilactone A.
• Authors of publication: Chaumont-Olive, Pauline; Maddaluno, Jacques; Harrison-Marchand, Anne
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2019
• Journal volume: 17
• Journal issue: 15
• Pages of publication: 3819 - 3824
• a: 12.4339 ± 0.0019 Å
• b: 19.941 ± 0.003 Å
• c: 12.721 ± 0.0019 Å
• α: 90°
• β: 96.173 ± 0.003°
• γ: 90°
• Cell volume: 3135.8 ± 0.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/a 1
• Hall space group symbol: -P 2yab
• Residual factor for all reflections: 0.1895
• Residual factor for significantly intense reflections: 0.0786
• Weighted residual factors for significantly intense reflections: 0.1887
• Weighted residual factors for all reflections included in the refinement: 0.2425
• Goodness-of-fit parameter for all reflections included in the refinement: 1.014
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No