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Information card for entry 7156855
Preview
Coordinates | 7156855.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C24 H21 N O2 S |
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Calculated formula | C24 H21 N O2 S |
Title of publication | A gold-catalyzed facile intramolecular rearrangement and cyclization sequence for synthesis of 2,5-dihydrofurans. |
Authors of publication | Sunil, Komalla; Thummala, Yadagiri; Dalovai, Purnachandar; Balasubramanian, Sridhar; Karunakar, Galla V. |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2019 |
Journal volume | 17 |
Journal issue | 24 |
Pages of publication | 6015 - 6024 |
a | 8.1 ± 0.001 Å |
b | 9.6228 ± 0.0012 Å |
c | 14.778 ± 0.0018 Å |
α | 98.898 ± 0.002° |
β | 99.647 ± 0.002° |
γ | 113.901 ± 0.002° |
Cell volume | 1006 ± 0.2 Å3 |
Cell temperature | 294 ± 2 K |
Ambient diffraction temperature | 294 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0923 |
Residual factor for significantly intense reflections | 0.0653 |
Weighted residual factors for significantly intense reflections | 0.1523 |
Weighted residual factors for all reflections included in the refinement | 0.1667 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.105 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7156855.html
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structural data.