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Information card for entry 7156947
Preview
Coordinates | 7156947.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C30 H26 F2 N4 O6 S2 |
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Calculated formula | C30 H26 F2 N4 O6 S2 |
Title of publication | Cu(i) catalysed annulation of isothiocyanates/isocyanates with 2-iodo-sulfonamides: synthesis of benzodithiazines, benzothiadiazinones, benzothiazinylidene-anilines and benzothiazolylidene-anilines. |
Authors of publication | Sandeep, K.; Siva Reddy, Alla; Kumara Swamy, K. C. |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2019 |
Journal volume | 17 |
Journal issue | 28 |
Pages of publication | 6880 - 6894 |
a | 12.557 ± 0.002 Å |
b | 18.579 ± 0.002 Å |
c | 13.015 ± 0.002 Å |
α | 90° |
β | 104.3 ± 0.019° |
γ | 90° |
Cell volume | 2942.3 ± 0.8 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.2423 |
Residual factor for significantly intense reflections | 0.1065 |
Weighted residual factors for significantly intense reflections | 0.2442 |
Weighted residual factors for all reflections included in the refinement | 0.3647 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.955 |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7156947.html
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