Crystallography Open Database

Information card for entry 7157033

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Coordinates	7157033.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C29 H24 N O4 P
Calculated formula	C29 H24 N O4 P
Title of publication	Regioselective radical arylation: silver-mediated synthesis of 3-phosphorylated coumarins, quinolin-2(1H)-one and benzophosphole oxides.
Authors of publication	Hou, Hong; Xu, Yue; Yang, Haibo; Yan, Chaoguo; Shi, Yaocheng; Zhu, Shaoqun
Journal of publication	Organic & biomolecular chemistry
Year of publication	2019
Journal volume	17
Journal issue	35
Pages of publication	8175 - 8184
a	22.6531 ± 0.001 Å
b	11.2558 ± 0.0004 Å
c	20.1149 ± 0.0009 Å
α	90°
β	105.379 ± 0.001°
γ	90°
Cell volume	4945.2 ± 0.4 Å³
Cell temperature	273.15 K
Ambient diffraction temperature	273.15 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1032
Residual factor for significantly intense reflections	0.0552
Weighted residual factors for significantly intense reflections	0.1239
Weighted residual factors for all reflections included in the refinement	0.1457
Goodness-of-fit parameter for all reflections included in the refinement	1.0759
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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