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Information card for entry 7157159
Preview
Coordinates | 7157159.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C24 H26 N2 O3 |
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Calculated formula | C24 H26 N2 O3 |
Title of publication | A gold-triggered dearomative spirocarbocyclization/Diels-Alder reaction cascade towards diverse bridged N-heterocycles. |
Authors of publication | He, Yi; Narmon, Thomas; Wu, Danjun; Li, Zhenghua; Van Meervelt, Luc; Van der Eycken, Erik V. |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2019 |
Journal volume | 17 |
Journal issue | 43 |
Pages of publication | 9529 |
a | 11.7236 ± 0.0005 Å |
b | 11.754 ± 0.0005 Å |
c | 17.2404 ± 0.0008 Å |
α | 73.252 ± 0.004° |
β | 73.789 ± 0.004° |
γ | 71.074 ± 0.004° |
Cell volume | 2106.24 ± 0.17 Å3 |
Cell temperature | 294.15 K |
Ambient diffraction temperature | 294.15 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.09 |
Residual factor for significantly intense reflections | 0.058 |
Weighted residual factors for significantly intense reflections | 0.123 |
Weighted residual factors for all reflections included in the refinement | 0.1407 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.044 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7157159.html
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Users of the data should acknowledge the original authors of the
structural data.