Expedient synthesis of highly substituted 3,4-dihydro-1,2-oxathiine 2,2-dioxides and 1,2-oxathiine 2,2-dioxides: revisiting sulfene additions to enaminoketones.
Authors of publication
Aiken, Stuart; Anozie, Kelechi; de Azevedo, Orlando D. C. C.; Cowen, Lewis; Edgar, Ross J. L.; Gabbutt, Christopher D.; Heron, B. Mark; Lawrence, Philippa A.; Mills, Abby J.; Rice, Craig R.; Urquhart, Mike W. J.; Zonidis, Dimitrios
Journal of publication
Organic & biomolecular chemistry
Year of publication
2019
Journal volume
17
Journal issue
44
Pages of publication
9585 - 9604
a
9.6018 ± 0.0007 Å
b
12.4113 ± 0.001 Å
c
16.8115 ± 0.0014 Å
α
90°
β
96.978 ± 0.003°
γ
90°
Cell volume
1988.6 ± 0.3 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 K
Number of distinct elements
5
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.0512
Residual factor for significantly intense reflections
0.0396
Weighted residual factors for significantly intense reflections
0.1011
Weighted residual factors for all reflections included in the refinement
0.1086
Goodness-of-fit parameter for all reflections included in the refinement
