Information card for entry 7157276

Structure parameters

• Formula: C32 H33 F N2 O6
• Calculated formula: C32 H33 F N2 O6
• Title of publication: Silver/palladium relay catalyzed 1,3-dipole annulation/allylation reactions to access fully substituted allyl imidazolidines.
• Authors of publication: Han, Ruiping; Ding, Yue; Jin, Xueke; Li, Er-Qing
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2020
• Journal volume: 18
• Journal issue: 4
• Pages of publication: 646 - 649
• a: 10.31491 ± 0.00015 Å
• b: 22.9483 ± 0.0003 Å
• c: 13.02398 ± 0.00018 Å
• α: 90°
• β: 101.4 ± 0.0014°
• γ: 90°
• Cell volume: 3022.08 ± 0.07 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0676
• Residual factor for significantly intense reflections: 0.0503
• Weighted residual factors for significantly intense reflections: 0.1388
• Weighted residual factors for all reflections included in the refinement: 0.1541
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No