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Information card for entry 7157290
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Coordinates | 7157290.cif |
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Original paper (by DOI) | HTML |
Formula | C29 H22 Cl N O2 S |
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Calculated formula | C29 H22 Cl N O2 S |
Title of publication | p-TsOH-mediated synthesis of substituted 2,4-diaryl-3-sulfonylquinolines from functionalized 2-aminobenzophenones and aromatic β-ketosulfones under microwave irradiation. |
Authors of publication | Chan, Chieh-Kai; Lai, Chien-Yu; Lo, Wei-Chih; Cheng, Yu-Ting; Chang, Meng-Yang; Wang, Cheng-Chung |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2020 |
Journal volume | 18 |
Journal issue | 2 |
Pages of publication | 305 - 315 |
a | 16.3487 ± 0.0018 Å |
b | 9.1325 ± 0.001 Å |
c | 16.747 ± 0.002 Å |
α | 90° |
β | 106.046 ± 0.003° |
γ | 90° |
Cell volume | 2403 ± 0.5 Å3 |
Cell temperature | 100 ± 0.2 K |
Ambient diffraction temperature | 100 ± 0.2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0396 |
Residual factor for significantly intense reflections | 0.0337 |
Weighted residual factors for significantly intense reflections | 0.0853 |
Weighted residual factors for all reflections included in the refinement | 0.0905 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.032 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7157290.html
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