Information card for entry 7157298

Structure parameters

• Chemical name: 5,5-dimethyl-12-phenylindolo[2,1-a]isoquinolin-6(5H)-one
• Formula: C24 H19 N O
• Calculated formula: C24 H19 N O
• Title of publication: Visible-light-induced intramolecular radical cascade of α-bromo-N-benzyl-alkylamides: a new strategy to synthesize tetracyclic N-fused indolo[2,1-a]isoquinolin-6(5H)-ones.
• Authors of publication: Gao, Xiaoshuang; Li, Chengyang; Yuan, Yao; Xie, Xiaomin; Zhang, Zhaoguo
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2020
• Journal volume: 18
• Journal issue: 2
• Pages of publication: 263 - 271
• a: 10.3896 ± 0.0008 Å
• b: 10.1601 ± 0.0012 Å
• c: 17.175 ± 0.003 Å
• α: 90°
• β: 102.57 ± 0.008°
• γ: 90°
• Cell volume: 1769.5 ± 0.4 ų
• Cell temperature: 301 ± 2 K
• Ambient diffraction temperature: 301 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0502
• Residual factor for significantly intense reflections: 0.0439
• Weighted residual factors for significantly intense reflections: 0.1152
• Weighted residual factors for all reflections included in the refinement: 0.1209
• Goodness-of-fit parameter for all reflections included in the refinement: 1.053
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No