Information card for entry 7157458

Structure parameters

• Formula: C10 H19 O2 Si
• Calculated formula: C10 H19 O2 Si
• Title of publication: Modular synthesis of oligoacetylacetones via site-selective silylation of acetylacetone derivatives.
• Authors of publication: Sarkar, Parantap; Inaba, Yuya; Shirakura, Hayato; Yoneda, Tomoki; Inokuma, Yasuhide
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2020
• Journal volume: 18
• Journal issue: 17
• Pages of publication: 3297 - 3302
• a: 7.1033 ± 0.0014 Å
• b: 15.7 ± 0.003 Å
• c: 10.748 ± 0.002 Å
• α: 90°
• β: 90.224 ± 0.006°
• γ: 90°
• Cell volume: 1198.6 ± 0.4 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.097
• Residual factor for significantly intense reflections: 0.0694
• Weighted residual factors for significantly intense reflections: 0.1738
• Weighted residual factors for all reflections included in the refinement: 0.1941
• Goodness-of-fit parameter for all reflections included in the refinement: 1.075
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No