Information card for entry 7157518
| Formula |
C22 H44 B10 O4 |
| Calculated formula |
C22 H44 B10 O4 |
| Title of publication |
Palladium-catalyzed regioselective synthesis of B(4,5)- or B(4)-substituted o-carboranes containing α,β-unsaturated carbonyls. |
| Authors of publication |
Zhang, Chuyi; Wang, Qian; Tian, Song; Zhang, Jianwei; Li, Jiaoyi; Zhou, Ling; Lu, Jian |
| Journal of publication |
Organic & biomolecular chemistry |
| Year of publication |
2020 |
| Journal volume |
18 |
| Journal issue |
25 |
| Pages of publication |
4723 - 4727 |
| a |
10.486 ± 0.005 Å |
| b |
11.704 ± 0.006 Å |
| c |
13.581 ± 0.007 Å |
| α |
87.493 ± 0.009° |
| β |
84.584 ± 0.008° |
| γ |
66.838 ± 0.007° |
| Cell volume |
1525.5 ± 1.3 Å3 |
| Cell temperature |
296 ± 2 K |
| Ambient diffraction temperature |
296 ± 2 K |
| Number of distinct elements |
4 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.112 |
| Residual factor for significantly intense reflections |
0.0835 |
| Weighted residual factors for significantly intense reflections |
0.2398 |
| Weighted residual factors for all reflections included in the refinement |
0.2813 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.046 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/7157518.html
