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Information card for entry 7157604
Preview
Coordinates | 7157604.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C21 H20 B F4 I O2 |
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Calculated formula | C21 H20 B F4 I O2 |
Title of publication | Fluorinations of unsymmetrical diaryliodonium salts containing ortho-sidearms; influence of sidearm on selectivity. |
Authors of publication | Abudken, Ahmed M. H.; Hope, Eric G.; Singh, Kuldip; Stuart, Alison M. |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2020 |
Journal volume | 18 |
Journal issue | 31 |
Pages of publication | 6140 - 6146 |
a | 12.965 ± 0.002 Å |
b | 11.911 ± 0.002 Å |
c | 13.389 ± 0.002 Å |
α | 90° |
β | 102.163 ± 0.003° |
γ | 90° |
Cell volume | 2021.2 ± 0.6 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0358 |
Residual factor for significantly intense reflections | 0.0308 |
Weighted residual factors for significantly intense reflections | 0.0735 |
Weighted residual factors for all reflections included in the refinement | 0.0758 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.033 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7157604.html
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Users of the data should acknowledge the original authors of the
structural data.