Information card for entry 7157705

Structure parameters

• Formula: C27 H20 N2 O8 S
• Calculated formula: C27 H20 N2 O8 S
• Title of publication: Stereoselective synthesis of dispiro heterocycles by [3 + 2] cycloaddition of azomethine ylides with a thiazolo[3,2-<i>a</i>]indole derivative.
• Authors of publication: Sathi, Vidya; Thomas, Noble V.; Deepthi, Ani
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2020
• Journal volume: 18
• Journal issue: 39
• Pages of publication: 7822 - 7826
• a: 7.6399 ± 0.0013 Å
• b: 11.119 ± 0.002 Å
• c: 15.958 ± 0.003 Å
• α: 70.281 ± 0.006°
• β: 78.966 ± 0.005°
• γ: 74.305 ± 0.005°
• Cell volume: 1221 ± 0.4 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0653
• Residual factor for significantly intense reflections: 0.0416
• Weighted residual factors for significantly intense reflections: 0.0945
• Weighted residual factors for all reflections included in the refinement: 0.1107
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No