Information card for entry 7157743

Structure parameters

• Formula: C37 H29 N O4
• Calculated formula: C37 H29 N O4
• Title of publication: Binaphthyl-based chiral ligands: design, synthesis and evaluation of their performance in enantioselective addition of diethylzinc to aromatic aldehydes.
• Authors of publication: Yao, Chao; Wu, Piao; Huang, Yue; Chen, Yaoqi; Li, Lin; Li, Yue-Ming
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2020
• Journal volume: 18
• Journal issue: 47
• Pages of publication: 9712 - 9725
• a: 10.7714 ± 0.0001 Å
• b: 11.3185 ± 0.0001 Å
• c: 13.3343 ± 0.0001 Å
• α: 66.429 ± 0.001°
• β: 80.647 ± 0.001°
• γ: 75.079 ± 0.001°
• Cell volume: 1436.53 ± 0.02 ų
• Cell temperature: 100 ± 0.13 K
• Ambient diffraction temperature: 100 ± 0.13 K
• Number of distinct elements: 4
• Space group number: 1
• Hermann-Mauguin space group symbol: P 1
• Hall space group symbol: P 1
• Residual factor for all reflections: 0.0266
• Residual factor for significantly intense reflections: 0.0261
• Weighted residual factors for significantly intense reflections: 0.0655
• Weighted residual factors for all reflections included in the refinement: 0.0658
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No