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Information card for entry 7157771
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Coordinates | 7157771.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | Zn-3c |
---|---|
Formula | C39 H53 Br N4 O4 Si3 Zn |
Calculated formula | C39 H53 Br N4 O4 Si3 Zn |
Title of publication | Central zinc metal-controlled regioselective meso-bromination of zincatedβ-silylporphyrins-rapid access to meso,β-dual-functionalized porphyrins. |
Authors of publication | Hayashi, Satoshi; Takamatsu, Rina; Takeda, Shiori; Noji, Masahiro; Takanami, Toshikatsu |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2020 |
Journal volume | 18 |
Journal issue | 48 |
Pages of publication | 9791 - 9795 |
a | 9.3441 Å |
b | 13.5093 Å |
c | 16.7025 Å |
α | 98.858° |
β | 102.47° |
γ | 91.92° |
Cell volume | 2029.23 Å3 |
Cell temperature | 93 K |
Ambient diffraction temperature | 93 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.2093 |
Residual factor for significantly intense reflections | 0.1381 |
Weighted residual factors for significantly intense reflections | 0.2792 |
Weighted residual factors for all reflections included in the refinement | 0.3577 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.046 |
Diffraction radiation wavelength | 1.54187 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7157771.html
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