Information card for entry 7157777

Structure parameters

• Formula: C23 H34 Cl N O2 Si
• Calculated formula: C23 H34 Cl N O2 Si
• Title of publication: Synthesis of spirocyclic heterocycles from α,β-unsaturated <i>N</i>-acyliminium ions.
• Authors of publication: Thaima, Thanphat; Yazici, Arife; Auranwiwat, Chiramet; Willis, Anthony C.; Wille, Uta; Limtharakul, Thunwadee; Pyne, Stephen G.
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2021
• Journal volume: 19
• Journal issue: 1
• Pages of publication: 259 - 272
• a: 9.2571 ± 0.0001 Å
• b: 8.0452 ± 0.0001 Å
• c: 16.5061 ± 0.0001 Å
• α: 90°
• β: 98.63 ± 0.0008°
• γ: 90°
• Cell volume: 1215.38 ± 0.02 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0403
• Residual factor for significantly intense reflections: 0.0401
• Weighted residual factors for all reflections: 0.1072
• Weighted residual factors for significantly intense reflections: 0.1066
• Weighted residual factors for all reflections included in the refinement: 0.1072
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0007
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No