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Information card for entry 7157854
Preview
Coordinates | 7157854.cif |
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Original paper (by DOI) | HTML |
Formula | C24 H20 O3 S |
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Calculated formula | C24 H20 O3 S |
Title of publication | Synthesis of C3-sulfone substituted naphthols <i>via</i> rhodium(III)-catalyzed annulation of sulfoxonium ylides with alkynylsulfones. |
Authors of publication | Xie, Wucheng; Jian, Xinyi; Zhang, Liyang; Jin, Kexin; Shi, Junjun; Zhu, Feng |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2021 |
Journal volume | 19 |
Journal issue | 7 |
Pages of publication | 1498 - 1502 |
a | 8.1695 ± 0.0006 Å |
b | 11.1838 ± 0.0009 Å |
c | 12.1869 ± 0.001 Å |
α | 116.288 ± 0.008° |
β | 102.125 ± 0.007° |
γ | 97.876 ± 0.006° |
Cell volume | 941.83 ± 0.16 Å3 |
Cell temperature | 99.98 ± 0.1 K |
Ambient diffraction temperature | 99.98 ± 0.1 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0546 |
Residual factor for significantly intense reflections | 0.0441 |
Weighted residual factors for significantly intense reflections | 0.1087 |
Weighted residual factors for all reflections included in the refinement | 0.1163 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.042 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7157854.html
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Users of the data should acknowledge the original authors of the
structural data.