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Information card for entry 7157856
Preview
Coordinates | 7157856.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C30 H34 N2 O3 |
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Calculated formula | C30 H34 N2 O3 |
Title of publication | Organocatalytic enantioselective [2 + 4]-annulation of γ-substituted allenoates with <i>N</i>-acyldiazenes for the synthesis of optically active 1,3,4-oxadiazines. |
Authors of publication | Guo, Xing; Chen, Xuling; Cheng, Yuyu; Chang, Xiaoyong; Li, Xuechen; Li, Pengfei |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2021 |
Journal volume | 19 |
Journal issue | 8 |
Pages of publication | 1727 - 1731 |
a | 10.6498 ± 0.0004 Å |
b | 10.95 ± 0.0004 Å |
c | 21.8176 ± 0.0008 Å |
α | 90° |
β | 104.078 ± 0.002° |
γ | 90° |
Cell volume | 2467.85 ± 0.16 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0389 |
Residual factor for significantly intense reflections | 0.0359 |
Weighted residual factors for significantly intense reflections | 0.0848 |
Weighted residual factors for all reflections included in the refinement | 0.0864 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.03 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7157856.html
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