Crystallography Open Database

Information card for entry 7158236

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Coordinates	7158236.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H22 N2 O5 S
Calculated formula	C24 H22 N2 O5 S
Title of publication	A zinc/PyBisulidine catalyzed asymmetric Mannich reaction of N-tosyl imines with 3-acyloxy-2-oxindoles
Authors of publication	Yang, Zinan; He, Huakang; Tian, Rui; Wu, Ruoran; Hu, Sheng; Wu, Yue; Zhou, Hui
Journal of publication	Organic & Biomolecular Chemistry
Year of publication	2021
Journal volume	19
Journal issue	34
Pages of publication	7460 - 7469
a	9.42743 ± 0.00015 Å
b	9.8509 ± 0.0002 Å
c	24.0927 ± 0.0004 Å
α	90°
β	90°
γ	90°
Cell volume	2237.46 ± 0.07 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0561
Residual factor for significantly intense reflections	0.0498
Weighted residual factors for significantly intense reflections	0.1295
Weighted residual factors for all reflections included in the refinement	0.1366
Goodness-of-fit parameter for all reflections included in the refinement	1.041
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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