Information card for entry 7158262

Structure parameters

• Formula: C33 H32 O
• Calculated formula: C33 H32 O
• Title of publication: TMSOTf-mediated synthesis of skipped dienes through the addition of olefins to imines and semicyclic <i>N</i>,<i>O</i>-acetals.
• Authors of publication: Feng, Yi-Man; Nie, Xiao-Di; Sun, Jian-Ting; Xu, Wen-Ke; Wei, Bang-Guo
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2021
• Journal volume: 19
• Journal issue: 36
• Pages of publication: 7883 - 7893
• a: 36.302 ± 0.008 Å
• b: 17.985 ± 0.004 Å
• c: 8.873 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5793 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293.06 K
• Number of distinct elements: 3
• Space group number: 60
• Hermann-Mauguin space group symbol: P b c n
• Hall space group symbol: -P 2n 2ab
• Residual factor for all reflections: 0.1704
• Residual factor for significantly intense reflections: 0.0989
• Weighted residual factors for significantly intense reflections: 0.2551
• Weighted residual factors for all reflections included in the refinement: 0.3205
• Goodness-of-fit parameter for all reflections included in the refinement: 0.995
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No