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Information card for entry 7158267
Preview
Coordinates | 7158267.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C13 H14 N2 O2 |
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Calculated formula | C13 H14 N2 O2 |
Title of publication | Copper(i)-catalyzed asymmetric intramolecular C-arylation with ureas as the additives: highly enantioselective formation of spirooxindoles |
Authors of publication | Ma, Haowen; Feng, Jiajie; Zhou, Wei; Chen, Chen; Deng, Zhuoji; Zhou, Fengtao; Ouyang, Yifan; Zhang, Xinhao; Cai, Qian |
Journal of publication | Organic & Biomolecular Chemistry |
Year of publication | 2021 |
Journal volume | 19 |
Journal issue | 34 |
Pages of publication | 7480 - 7484 |
a | 6.956 ± 0.0002 Å |
b | 8.4636 ± 0.0003 Å |
c | 19.6496 ± 0.0006 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 1156.83 ± 0.06 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 4 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0374 |
Residual factor for significantly intense reflections | 0.0366 |
Weighted residual factors for significantly intense reflections | 0.0984 |
Weighted residual factors for all reflections included in the refinement | 0.0993 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.055 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7158267.html
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