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Information card for entry 7158454
Preview
Coordinates | 7158454.cif |
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Original paper (by DOI) | HTML |
Common name | Tetrahydrochromeno[4,3-b]pyrrole |
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Chemical name | dimethyl (E)-3-styryl-1,2,3,9b-tetrahydrochromeno[4,3-b]pyrrole-2,3a(4H)-dicarboxylate |
Formula | C7 H0 N16 O6 |
Calculated formula | C23 H23 N O5 |
Title of publication | Azomethine ylide cycloaddition of 1,3-dienyl esters: highly regio- and diastereoselective synthesis of functionalized pyrrolidinochromenes. |
Authors of publication | Bakthadoss, Manickam; Mushaf, Mohammad; Agarwal, Vishal; Reddy, Tadiparthi Thirupathi; Sharada, Duddu S. |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2022 |
Journal volume | 20 |
Journal issue | 4 |
Pages of publication | 778 - 782 |
a | 12.2643 ± 0.0009 Å |
b | 7.5844 ± 0.0006 Å |
c | 21.7321 ± 0.0016 Å |
α | 90° |
β | 95.637 ± 0.007° |
γ | 90° |
Cell volume | 2011.7 ± 0.3 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.1011 |
Residual factor for significantly intense reflections | 0.0606 |
Weighted residual factors for significantly intense reflections | 0.1565 |
Weighted residual factors for all reflections included in the refinement | 0.1819 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.07 |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7158454.html
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