Information card for entry 7158474

Structure parameters

• Formula: C18 H29 N O Si
• Calculated formula: C18 H29 N O Si
• Title of publication: Copper-Promoted Difunctionalization of Unactivated Alkenes with Silanes
• Authors of publication: Xue, Yingying; Guo, Zhuangzhuang; Chen, Xiaoyu; Li, Jingya; Zou, Dapeng; Wu, Yangjie; Wu, Yusheng
• Journal of publication: Organic & Biomolecular Chemistry
• Year of publication: 2022
• a: 22.3463 ± 0.0008 Å
• b: 7.5222 ± 0.0003 Å
• c: 22.4194 ± 0.0011 Å
• α: 90°
• β: 102.133 ± 0.004°
• γ: 90°
• Cell volume: 3684.4 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0606
• Residual factor for significantly intense reflections: 0.047
• Weighted residual factors for significantly intense reflections: 0.1276
• Weighted residual factors for all reflections included in the refinement: 0.1415
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No