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Information card for entry 7158505
Preview
Coordinates | 7158505.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C27 H30 N2 O2 S |
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Calculated formula | C27 H30 N2 O2 S |
Title of publication | Enantioselective synthesis of 2-indolyl methanamine derivatives through disulfonimide-catalyzed Friedel-Crafts C2-alkylation of 3-substituted indoles with imines. |
Authors of publication | Sun, Peng; Jia, Zi-Hao; Tang, Li; Zheng, Hao; Li, Zhang-Rui; Chen, Ling-Yan; Li, Ya |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2022 |
Journal volume | 20 |
Journal issue | 9 |
Pages of publication | 1916 - 1925 |
a | 9.4321 ± 0.0003 Å |
b | 14.6668 ± 0.0005 Å |
c | 17.7584 ± 0.0006 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 2456.67 ± 0.14 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 5 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0393 |
Residual factor for significantly intense reflections | 0.0338 |
Weighted residual factors for significantly intense reflections | 0.0831 |
Weighted residual factors for all reflections included in the refinement | 0.0871 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.065 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7158505.html
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Users of the data should acknowledge the original authors of the
structural data.