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Information card for entry 7158507
Preview
Coordinates | 7158507.cif |
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Original paper (by DOI) | HTML |
Chemical name | 2,6-dimesityl-1-methyl-4-phenyl-1,4-dihydropyridine |
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Formula | C30 H33 N |
Calculated formula | C30 H33 N |
Title of publication | A strong hydride donating, acid stable and reusable 1,4-dihydropyridine for selective aldimine and aldehyde reductions. |
Authors of publication | Hirao, Yasukazu; Eto, Hajime; Teraoka, Mitsuru; Kubo, Takashi |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2022 |
Journal volume | 20 |
Journal issue | 8 |
Pages of publication | 1671 - 1679 |
a | 12.0239 ± 0.001 Å |
b | 14.1732 ± 0.0012 Å |
c | 17.0536 ± 0.0015 Å |
α | 107.498 ± 0.008° |
β | 103.65 ± 0.007° |
γ | 107.038 ± 0.008° |
Cell volume | 2477.1 ± 0.5 Å3 |
Cell temperature | 200 ± 2 K |
Ambient diffraction temperature | 200.15 K |
Number of distinct elements | 3 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1359 |
Residual factor for significantly intense reflections | 0.0688 |
Weighted residual factors for significantly intense reflections | 0.1544 |
Weighted residual factors for all reflections included in the refinement | 0.1831 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.019 |
Diffraction radiation wavelength | 0.71075 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7158507.html
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