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Information card for entry 7158509
Preview
Coordinates | 7158509.cif |
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Original paper (by DOI) | HTML |
Formula | C41 H45 N O3 Si |
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Calculated formula | C41 H45 N O3 Si |
Title of publication | A case study of the MAC (masked acyl cyanide) oxyhomologation of <i>N</i>,<i>N</i>-dibenzyl-L-phenylalaninal with <i>anti</i> diastereoselectivity: preparation of (2<i>S</i>,3<i>S</i>)-allophenylnorstatin esters. |
Authors of publication | He, Xuefeng; Buchotte, Marie; Guillot, Régis; Deloisy, Sandrine; Aitken, David J. |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2022 |
Journal volume | 20 |
Journal issue | 8 |
Pages of publication | 1769 - 1781 |
a | 10.8331 ± 0.0004 Å |
b | 24.5894 ± 0.001 Å |
c | 13.8643 ± 0.0005 Å |
α | 90° |
β | 107.06 ± 0.001° |
γ | 90° |
Cell volume | 3530.7 ± 0.2 Å3 |
Cell temperature | 100 ± 1 K |
Ambient diffraction temperature | 100 ± 1 K |
Number of distinct elements | 5 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0318 |
Residual factor for significantly intense reflections | 0.0308 |
Weighted residual factors for significantly intense reflections | 0.0787 |
Weighted residual factors for all reflections included in the refinement | 0.0793 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.024 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7158509.html
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