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Information card for entry 7158513
Preview
Coordinates | 7158513.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C24 H18 F N O4 S |
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Calculated formula | C24 H18 F N O4 S |
Title of publication | Rh(III)-Catalyzed C-H bond activation/annulation reactions of arylacyl ammonium salts with 4-diazoisochroman-3-imines and 4-diazoisoquinolin-3-ones. |
Authors of publication | Suleman, Muhammad; Qi, Minghui; Xie, Jianwei; Lu, Ping; Wang, Yanguang |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2022 |
Journal volume | 20 |
Journal issue | 9 |
Pages of publication | 1900 - 1906 |
a | 7.1439 ± 0.0014 Å |
b | 10.734 ± 0.002 Å |
c | 14.451 ± 0.003 Å |
α | 72.259 ± 0.009° |
β | 81.41 ± 0.009° |
γ | 72.811 ± 0.01° |
Cell volume | 1006.2 ± 0.4 Å3 |
Cell temperature | 170 ± 2 K |
Ambient diffraction temperature | 170 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0337 |
Residual factor for significantly intense reflections | 0.0322 |
Weighted residual factors for significantly intense reflections | 0.0858 |
Weighted residual factors for all reflections included in the refinement | 0.0871 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.043 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7158513.html
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structural data.