Information card for entry 7158570

Structure parameters

• Formula: C24 H21 F2 N O
• Calculated formula: C24 H21 F2 N O
• Title of publication: Co-catalyzed atom transfer radical addition of bromodifluoroacetamides, expanding the scope of radical alkylation
• Authors of publication: Yamamoto, Yoshihiko; Suzuki, Harufumi; Kuroyanagi, Eisuke; Yamada, Keiji; Yasui, Takeshi
• Journal of publication: Organic & Biomolecular Chemistry
• Year of publication: 2022
• a: 10.2403 ± 0.0005 Å
• b: 15.5996 ± 0.0008 Å
• c: 12.3812 ± 0.0006 Å
• α: 90°
• β: 102.08 ± 0.007°
• γ: 90°
• Cell volume: 1934.03 ± 0.17 ų
• Cell temperature: 296 K
• Ambient diffraction temperature: 296 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0519
• Residual factor for significantly intense reflections: 0.0481
• Weighted residual factors for significantly intense reflections: 0.1211
• Weighted residual factors for all reflections included in the refinement: 0.1243
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation wavelength: 1.54187 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No