Information card for entry 7158574
Formula |
C26 H37 B O P |
Calculated formula |
C26 H37 B O P |
Title of publication |
The stereoselective conversion of epimerized alkoxyl phosphine–borane to P,C, axial-stereogenic tertiary phosphine via cleavage of P–O bond |
Authors of publication |
Zhai, De-Hua; Yan, Bing-Xia; Li, Zhan-Cai; Lin, Zhu; Li, Qiang; Wang, Yan-Lan; Zheng, Hong-Xing; Zhao, Chang-Qiu |
Journal of publication |
Organic & Biomolecular Chemistry |
Year of publication |
2022 |
a |
12.84 ± 0.05 Å |
b |
13.69 ± 0.05 Å |
c |
14.68 ± 0.05 Å |
α |
90° |
β |
90° |
γ |
90° |
Cell volume |
2580 ± 16 Å3 |
Cell temperature |
298.15 K |
Ambient diffraction temperature |
298.15 K |
Number of distinct elements |
5 |
Space group number |
19 |
Hermann-Mauguin space group symbol |
P 21 21 21 |
Hall space group symbol |
P 2ac 2ab |
Residual factor for all reflections |
0.2276 |
Residual factor for significantly intense reflections |
0.1183 |
Weighted residual factors for significantly intense reflections |
0.2873 |
Weighted residual factors for all reflections included in the refinement |
0.35 |
Goodness-of-fit parameter for all reflections included in the refinement |
0.965 |
Diffraction radiation wavelength |
0.71073 Å |
Diffraction radiation type |
MoKα |
Has coordinates |
Yes |
Has disorder |
No |
Has Fobs |
No |
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The link is:
https://www.crystallography.net/7158574.html