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Information card for entry 7158649
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Coordinates | 7158649.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | 1,1,2,2-tetramethyl-cyclobuta-quinolin-3(1H)-one |
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Formula | C15 H19 N O |
Calculated formula | C15 H19 N O |
Title of publication | Enantioselective [2 + 2] photocycloaddition of quinolone using a <i>C</i><sub>1</sub>-symmetric chiral phosphoric acid as a visible-light photocatalyst. |
Authors of publication | Takagi, Ryukichi; Tanimoto, Takaaki |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2022 |
Journal volume | 20 |
Journal issue | 19 |
Pages of publication | 3940 - 3947 |
a | 7.1151 ± 0.0001 Å |
b | 8.4448 ± 0.0001 Å |
c | 21.3264 ± 0.0002 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 1281.41 ± 0.03 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100 K |
Number of distinct elements | 4 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0304 |
Residual factor for significantly intense reflections | 0.0295 |
Weighted residual factors for significantly intense reflections | 0.0765 |
Weighted residual factors for all reflections included in the refinement | 0.0773 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.02 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7158649.html
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