Information card for entry 7158660

Structure parameters

• Formula: C22 H23 N O3
• Calculated formula: C22 H23 N O3
• Title of publication: Synthesis of spirocyclic oxazole derivatives from 2-arylidene cycloalkanones and α-halohydroxamates
• Authors of publication: Wan, Huiyang; Xia, Shuangshuang; Liu, Xinghua; Jian, Yongchan; An, Yuanyuan; Wang, Yubin
• Journal of publication: Organic & Biomolecular Chemistry
• Year of publication: 2022
• a: 36.572 ± 0.004 Å
• b: 5.7581 ± 0.0006 Å
• c: 18.4236 ± 0.0019 Å
• α: 90°
• β: 106.802 ± 0.003°
• γ: 90°
• Cell volume: 3714.1 ± 0.7 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296.15 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.065
• Residual factor for significantly intense reflections: 0.0471
• Weighted residual factors for significantly intense reflections: 0.1103
• Weighted residual factors for all reflections included in the refinement: 0.1209
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No