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Information card for entry 7158699
Preview
Coordinates | 7158699.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C21 H14 N2 |
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Calculated formula | C21 H14 N2 |
Title of publication | A direct entry to polycyclic quinoxaline derivatives <i>via</i> I<sub>2</sub>-DMSO mediated oxidative decarboxylation of α-amino acids and the subsequent Pictet-Spengler cyclization reaction. |
Authors of publication | Samanta, Surya Kanta; Sarkar, Rumpa; Sengupta, Utsav; Das, Sayan; Ganguly, Debabani; Hasija, Avantika; Chopra, Deepak; Bera, Mrinal K. |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2022 |
Journal volume | 20 |
Journal issue | 22 |
Pages of publication | 4650 - 4658 |
a | 4.0812 ± 0.0008 Å |
b | 17.973 ± 0.003 Å |
c | 19.807 ± 0.004 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 1452.9 ± 0.5 Å3 |
Cell temperature | 293.31 K |
Ambient diffraction temperature | 293.31 K |
Number of distinct elements | 3 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.1222 |
Residual factor for significantly intense reflections | 0.0981 |
Weighted residual factors for significantly intense reflections | 0.2533 |
Weighted residual factors for all reflections included in the refinement | 0.2696 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.102 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7158699.html
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