Information card for entry 7158701

Structure parameters

• Formula: C24 H34 Li2 N2 O4
• Calculated formula: C24 H34 Li2 N2 O4
• Title of publication: A facile approach to C-functionalized β-ketoimine compounds via terminal alkylation of a tetralithiated intermediate
• Authors of publication: Zhou, Shuai; Xu, Xiaojuan; Zhu, Xu; Zheng, Yu; Chen, Sufang; Xue, Mingqiang
• Journal of publication: Organic & Biomolecular Chemistry
• Year of publication: 2022
• a: 10.4007 ± 0.0011 Å
• b: 13.6605 ± 0.0015 Å
• c: 17.5771 ± 0.0019 Å
• α: 99.394 ± 0.003°
• β: 94.887 ± 0.003°
• γ: 93.08 ± 0.003°
• Cell volume: 2449.1 ± 0.5 ų
• Cell temperature: 128.01 K
• Ambient diffraction temperature: 128.01 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1825
• Residual factor for significantly intense reflections: 0.0969
• Weighted residual factors for significantly intense reflections: 0.2569
• Weighted residual factors for all reflections included in the refinement: 0.3327
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No