Information card for entry 7158835
Formula |
C27 H22 Br Cl2 N O3 |
Calculated formula |
C27 H22 Br Cl2 N O3 |
Title of publication |
The polychloromethylation/acyloxylation of 1,6-enynes with chloroalkanes and diacyl peroxides through dual-role designs |
Authors of publication |
Zhang, Jun-Hao; Jiang, Li-Lin; Hu, Sen-Jie; Li, Jiao-Zhe; Yu, Xuan-Chi; Liu, Fa-Liang; Guan, Yu-Tao; Lei, Ke-Wei; Wei, Wen-Ting |
Journal of publication |
Organic & Biomolecular Chemistry |
Year of publication |
2022 |
a |
12.3719 ± 0.0009 Å |
b |
11.052 ± 0.0009 Å |
c |
18.6624 ± 0.0014 Å |
α |
90° |
β |
103.575 ± 0.002° |
γ |
90° |
Cell volume |
2480.5 ± 0.3 Å3 |
Cell temperature |
170 K |
Ambient diffraction temperature |
170 K |
Number of distinct elements |
6 |
Space group number |
14 |
Hermann-Mauguin space group symbol |
P 1 21/c 1 |
Hall space group symbol |
-P 2ybc |
Residual factor for all reflections |
0.0934 |
Residual factor for significantly intense reflections |
0.0425 |
Weighted residual factors for significantly intense reflections |
0.0799 |
Weighted residual factors for all reflections included in the refinement |
0.0973 |
Goodness-of-fit parameter for all reflections included in the refinement |
1.005 |
Diffraction radiation wavelength |
0.71073 Å |
Diffraction radiation type |
MoKα |
Has coordinates |
Yes |
Has disorder |
No |
Has Fobs |
No |
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The link is:
https://www.crystallography.net/7158835.html