Information card for entry 7158973

Structure parameters

• Formula: C32 H25 N O2
• Calculated formula: C32 H25 N O2
• Title of publication: Rhodium Catalysed Intramolecular Benzannulation for the Formation of Tetracyclic Carbazoles
• Authors of publication: Kumar, Y. Bharath Chaithanya; Samatha, Polasani; Mainkar, Prathama S.; Adepu, Raju
• Journal of publication: Organic & Biomolecular Chemistry
• Year of publication: 2022
• a: 8.2394 ± 0.0004 Å
• b: 10.079 ± 0.0006 Å
• c: 15.9028 ± 0.0008 Å
• α: 79.577 ± 0.002°
• β: 77.886 ± 0.002°
• γ: 69.796 ± 0.002°
• Cell volume: 1203.3 ± 0.11 ų
• Cell temperature: 294 ± 2 K
• Ambient diffraction temperature: 294 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1614
• Residual factor for significantly intense reflections: 0.0597
• Weighted residual factors for significantly intense reflections: 0.1541
• Weighted residual factors for all reflections included in the refinement: 0.1979
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No