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Information card for entry 7159091
Preview
Coordinates | 7159091.cif |
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Original paper (by DOI) | HTML |
Formula | C29 H24 F3 N3 |
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Calculated formula | C29 H24 F3 N3 |
Title of publication | The B(C<sub>6</sub>F<sub>5</sub>)<sub>3</sub>·H<sub>2</sub>O promoted synthesis of fluoroalkylated 3,3',3''-trisindolylmethanes from fluorocarboxylic acids and indoles. |
Authors of publication | Xu, Xin; Gao, Dandan; Wang, Jiahua; Tang, Xiang-Ying; Wang, Long |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2023 |
Journal volume | 21 |
Journal issue | 7 |
Pages of publication | 1478 - 1486 |
a | 8.86737 ± 0.00003 Å |
b | 15.02535 ± 0.00006 Å |
c | 17.36072 ± 0.00007 Å |
α | 90° |
β | 91.6634 ± 0.0003° |
γ | 90° |
Cell volume | 2312.09 ± 0.015 Å3 |
Cell temperature | 99.99 ± 0.1 K |
Ambient diffraction temperature | 99.99 ± 0.1 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0381 |
Residual factor for significantly intense reflections | 0.0377 |
Weighted residual factors for significantly intense reflections | 0.0925 |
Weighted residual factors for all reflections included in the refinement | 0.0928 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.073 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7159091.html
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structural data.