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Information card for entry 7159186
Preview
Coordinates | 7159186.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C26 H22 O8 S |
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Calculated formula | C26 H22 O8 S |
Title of publication | One-pot synthesis of sulfonyl dibenzosuberdiones <i>via</i> In(OTf)<sub>3</sub>-promoted double Friedel-Crafts reactions of oxygenated arylacetic acids with β-arylvinyl sulfones. |
Authors of publication | Chang, Meng-Yang; Lin, Chun-Yi |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2023 |
Journal volume | 21 |
Journal issue | 11 |
Pages of publication | 2405 - 2416 |
a | 7.8698 ± 0.0002 Å |
b | 8.091 ± 0.0002 Å |
c | 18.4031 ± 0.0004 Å |
α | 97.31 ± 0.002° |
β | 90.418 ± 0.002° |
γ | 109.486 ± 0.003° |
Cell volume | 1094.16 ± 0.05 Å3 |
Cell temperature | 113 ± 2 K |
Ambient diffraction temperature | 113 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0457 |
Residual factor for significantly intense reflections | 0.0401 |
Weighted residual factors for significantly intense reflections | 0.1012 |
Weighted residual factors for all reflections included in the refinement | 0.1042 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.046 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7159186.html
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Users of the data should acknowledge the original authors of the
structural data.