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Information card for entry 7159198
Preview
Coordinates | 7159198.cif |
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Original paper (by DOI) | HTML |
Formula | C42 H43 Cl2 N O S |
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Calculated formula | C41 H40 N O S |
Title of publication | Construction of heterocycle-fused tetrahydrocarbazoles through a formal [3 + 3]-annulation of 2-indolylmethanols with <i>para</i>-quinone methides. |
Authors of publication | Singh, Gurdeep; Sharma, Sonam; Pandey, Rajat; Rekha, ?; Vijaya Anand, Ramasamy |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2023 |
Journal volume | 21 |
Journal issue | 12 |
Pages of publication | 2493 - 2498 |
a | 9.2987 ± 0.0004 Å |
b | 12.1896 ± 0.0005 Å |
c | 17.6436 ± 0.0008 Å |
α | 109.223 ± 0.004° |
β | 90.262 ± 0.004° |
γ | 104.83 ± 0.004° |
Cell volume | 1816.78 ± 0.15 Å3 |
Cell temperature | 298 ± 0.1 K |
Ambient diffraction temperature | 298 ± 0.1 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0754 |
Residual factor for significantly intense reflections | 0.0575 |
Weighted residual factors for significantly intense reflections | 0.1586 |
Weighted residual factors for all reflections included in the refinement | 0.1808 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.064 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7159198.html
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Users of the data should acknowledge the original authors of the
structural data.