Information card for entry 7159257

Structure parameters

• Formula: C50 H62 O10 P2
• Calculated formula: C50 H62 O10 P2
• Title of publication: Nickel-catalysed enantioselective reaction of secondary phosphine oxides and activated vinylcyclopropanes.
• Authors of publication: Huang, Zhuo; Liu, Xu-Teng; Cui, Ranran; Zhang, Qing-Wei
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2023
• Journal volume: 21
• Journal issue: 15
• Pages of publication: 3096 - 3100
• a: 5.37551 ± 0.00009 Å
• b: 7.85484 ± 0.00012 Å
• c: 56.3649 ± 0.0009 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2379.94 ± 0.07 ų
• Cell temperature: 100.01 ± 0.1 K
• Ambient diffraction temperature: 100.01 ± 0.1 K
• Number of distinct elements: 4
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0988
• Residual factor for significantly intense reflections: 0.0953
• Weighted residual factors for significantly intense reflections: 0.2373
• Weighted residual factors for all reflections included in the refinement: 0.2409
• Goodness-of-fit parameter for all reflections included in the refinement: 1.094
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No