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Information card for entry 7159287
Preview
Coordinates | 7159287.cif |
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Original paper (by DOI) | HTML |
Formula | C18 H24 N2 O6 |
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Calculated formula | C18 H24 N2 O6 |
Title of publication | Cyclization of <i>N</i>-Boc-(<i>E</i>)-α,β-unsaturated γ-amino acid active esters into <i>N</i>-Boc-(<i>Z</i>)-α,β-unsaturated γ-lactams through <i>E</i> → <i>Z</i> isomerization. |
Authors of publication | Singh, Manjeet; Kumar, Manish; Nalawade, Sachin A.; Puneeth Kumar, DRGKoppalu R; Gopi, Hosahudya N. |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2023 |
Journal volume | 21 |
Journal issue | 18 |
Pages of publication | 3766 - 3769 |
a | 6.216 ± 0.003 Å |
b | 5.362 ± 0.003 Å |
c | 28.415 ± 0.013 Å |
α | 90° |
β | 95.424 ± 0.012° |
γ | 90° |
Cell volume | 942.8 ± 0.8 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 4 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.1436 |
Residual factor for significantly intense reflections | 0.0899 |
Weighted residual factors for significantly intense reflections | 0.211 |
Weighted residual factors for all reflections included in the refinement | 0.2324 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.085 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7159287.html
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