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Information card for entry 7159290
Preview
Coordinates | 7159290.cif |
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Original paper (by DOI) | HTML |
Formula | C16 H19 N O3 |
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Calculated formula | C16 H19 N O3 |
Title of publication | Cyclization of <i>N</i>-Boc-(<i>E</i>)-α,β-unsaturated γ-amino acid active esters into <i>N</i>-Boc-(<i>Z</i>)-α,β-unsaturated γ-lactams through <i>E</i> → <i>Z</i> isomerization. |
Authors of publication | Singh, Manjeet; Kumar, Manish; Nalawade, Sachin A.; Puneeth Kumar, DRGKoppalu R; Gopi, Hosahudya N. |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2023 |
Journal volume | 21 |
Journal issue | 18 |
Pages of publication | 3766 - 3769 |
a | 6.146 ± 0.003 Å |
b | 14.129 ± 0.007 Å |
c | 16.674 ± 0.008 Å |
α | 90° |
β | 99.499 ± 0.014° |
γ | 90° |
Cell volume | 1428.1 ± 1.2 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.1915 |
Residual factor for significantly intense reflections | 0.0723 |
Weighted residual factors for significantly intense reflections | 0.1772 |
Weighted residual factors for all reflections included in the refinement | 0.271 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.79 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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