Information card for entry 7159321

Structure parameters

• Chemical name: (R)-6d
• Formula: C11 H12 O3
• Calculated formula: C11 H12 O3
• Title of publication: An expedient copper-catalysed asymmetric synthesis of γ-lactones and γ-lactams. Application to the synthesis of lucidulactone A.
• Authors of publication: Ojo, O. Stephen; Hughes, David L.; Richards, Christopher J.
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2023
• Journal volume: 21
• Journal issue: 19
• Pages of publication: 4144 - 4149
• a: 7.0003 ± 0.0005 Å
• b: 7.5875 ± 0.0003 Å
• c: 9.1343 ± 0.0007 Å
• α: 90°
• β: 106.874 ± 0.007°
• γ: 90°
• Cell volume: 464.28 ± 0.05 ų
• Cell temperature: 102 ± 4 K
• Ambient diffraction temperature: 100.01 ± 0.1 K
• Number of distinct elements: 3
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.042
• Residual factor for significantly intense reflections: 0.0418
• Weighted residual factors for significantly intense reflections: 0.1152
• Weighted residual factors for all reflections included in the refinement: 0.1154
• Goodness-of-fit parameter for all reflections included in the refinement: 1.071
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No