Information card for entry 7159324

Structure parameters

• Formula: C25 H23 N Si
• Calculated formula: C25 H23 N Si
• Title of publication: NHC-Zn alkyl catalyzed cross-dehydrocoupling of amines and silanes.
• Authors of publication: Harinath, Adimulam; Karmakar, Himadri; Kisan, Devadkar Ajitaro; Nayek, Hari Pada; Panda, Tarun K.
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2023
• Journal volume: 21
• Journal issue: 20
• Pages of publication: 4237 - 4244
• a: 6.8198 ± 0.0002 Å
• b: 11.6463 ± 0.0004 Å
• c: 12.6683 ± 0.0005 Å
• α: 90°
• β: 99.955 ± 0.003°
• γ: 90°
• Cell volume: 991.04 ± 0.06 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0547
• Residual factor for significantly intense reflections: 0.0532
• Weighted residual factors for significantly intense reflections: 0.1464
• Weighted residual factors for all reflections included in the refinement: 0.1483
• Goodness-of-fit parameter for all reflections included in the refinement: 1.1
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No