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Information card for entry 7159329
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Coordinates | 7159329.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | Ray |
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Formula | C23 H16 F O2 |
Calculated formula | C23 H17 F O2 |
Title of publication | Electronically-controlled diastereoselective synthesis of spirocycles <i>via</i> [4 + 2] cycloaddition of 2-arylidene-1-indenones with benzyne. |
Authors of publication | Ray, Subhasish; Yadav, Anup Kumar; Singh, Saurabh; Ansari, Monish Arbaz; Singh, Maya Shankar |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2023 |
Journal volume | 21 |
Journal issue | 20 |
Pages of publication | 4195 - 4199 |
a | 8.03311 ± 0.0001 Å |
b | 24.9979 ± 0.0003 Å |
c | 8.69995 ± 0.0001 Å |
α | 90° |
β | 99.4412 ± 0.0012° |
γ | 90° |
Cell volume | 1723.38 ± 0.04 Å3 |
Cell temperature | 293 K |
Ambient diffraction temperature | 293 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0498 |
Residual factor for significantly intense reflections | 0.0462 |
Weighted residual factors for significantly intense reflections | 0.1183 |
Weighted residual factors for all reflections included in the refinement | 0.1221 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.09 |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7159329.html
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