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Information card for entry 7159547
Preview
Coordinates | 7159547.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C17 H14 N2 O2 |
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Calculated formula | C17 H14 N2 O2 |
Title of publication | Regioselective <i>ortho</i> C-H insertion of <i>N</i>-nitrosoanilines with naphthoquinone carbenes. |
Authors of publication | Peng, Rui-Jun; Chen, Yuan; Zhang, Xue-Jing; Yan, Ming |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2023 |
Journal volume | 21 |
Journal issue | 37 |
Pages of publication | 7525 - 7529 |
a | 11.3559 ± 0.0004 Å |
b | 8.1137 ± 0.0002 Å |
c | 16.0334 ± 0.0004 Å |
α | 90° |
β | 101.324 ± 0.003° |
γ | 90° |
Cell volume | 1448.53 ± 0.07 Å3 |
Cell temperature | 100 ± 0.1 K |
Ambient diffraction temperature | 100 ± 0.1 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0483 |
Residual factor for significantly intense reflections | 0.0429 |
Weighted residual factors for significantly intense reflections | 0.1177 |
Weighted residual factors for all reflections included in the refinement | 0.1226 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.079 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7159547.html
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Users of the data should acknowledge the original authors of the
structural data.