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Information card for entry 7159565
Preview
Coordinates | 7159565.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C26 H22 O4 |
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Calculated formula | C26 H22 O4 |
Title of publication | Selective electrophilic cyclization of <i>ortho</i>-carbonylarylacetylenols for the synthesis of cyclopenta[<i>a</i>]naphthalenol and 2-phenylnaphthalen-1-ol analogs. |
Authors of publication | Jantrapirom, Jantra; Yongpanich, Phornphan; Tummatorn, Jumreang; Chainok, Kittipong; Jiajaroen, Suwadee; Thongsornkleeb, Charnsak; Ruchirawat, Somsak |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2023 |
Journal volume | 21 |
Journal issue | 42 |
Pages of publication | 8500 - 8515 |
a | 8.672 ± 0.002 Å |
b | 10.126 ± 0.003 Å |
c | 12.865 ± 0.004 Å |
α | 80.213 ± 0.01° |
β | 76.589 ± 0.009° |
γ | 67.977 ± 0.009° |
Cell volume | 1014.4 ± 0.5 Å3 |
Cell temperature | 296 K |
Ambient diffraction temperature | 296 K |
Number of distinct elements | 3 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0917 |
Residual factor for significantly intense reflections | 0.0732 |
Weighted residual factors for significantly intense reflections | 0.1588 |
Weighted residual factors for all reflections included in the refinement | 0.1683 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.099 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Diffraction radiation X-ray symbol | K-L~3~ |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7159565.html
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Users of the data should acknowledge the original authors of the
structural data.