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Information card for entry 7159581
Preview
Coordinates | 7159581.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C21 H19 N O3 |
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Calculated formula | C21 H19 N O3 |
Title of publication | Regioselective [2 + 1] photocycloaddition of 2-pyridones with diazo compounds. |
Authors of publication | He, Fengya; Sun, Ziyi; Li, Chenyue; Jiang, Zibin; Miao, Hui; Li, Qinglin; Wu, Chenggui |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2023 |
Journal volume | 21 |
Journal issue | 41 |
Pages of publication | 8273 - 8278 |
a | 11.0203 ± 0.0006 Å |
b | 12.3994 ± 0.0006 Å |
c | 13.7932 ± 0.0008 Å |
α | 90° |
β | 110.799 ± 0.006° |
γ | 90° |
Cell volume | 1761.95 ± 0.18 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0767 |
Residual factor for significantly intense reflections | 0.0564 |
Weighted residual factors for significantly intense reflections | 0.1754 |
Weighted residual factors for all reflections included in the refinement | 0.192 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.055 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7159581.html
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structural data.