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Information card for entry 7159588
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Coordinates | 7159588.cif |
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Original paper (by DOI) | HTML |
Formula | C27 H25 Cl N2 O4 S |
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Calculated formula | C27 H25 Cl N2 O4 S |
Title of publication | Palladium-catalyzed decarboxylative α-allylation of thiazolidinones and azlactones with sulfonamido-substituted acyclic allylic carbonates. |
Authors of publication | Rao, Han-Wen; Zhao, Tian-Lan; Wang, Long; Deng, Hong-Dan; Zhang, Yan-Ping; You, Yong; Wang, Zhen-Hua; Zhao, Jian-Qiang; Yuan, Wei-Cheng |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2023 |
Journal volume | 21 |
Journal issue | 42 |
Pages of publication | 8593 - 8602 |
a | 10.1642 ± 0.0002 Å |
b | 11.1077 ± 0.0002 Å |
c | 12.6071 ± 0.0002 Å |
α | 67.633 ± 0.002° |
β | 85.524 ± 0.001° |
γ | 70.287 ± 0.002° |
Cell volume | 1237.05 ± 0.05 Å3 |
Cell temperature | 99.98 ± 0.1 K |
Ambient diffraction temperature | 99.98 ± 0.1 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0373 |
Residual factor for significantly intense reflections | 0.0365 |
Weighted residual factors for significantly intense reflections | 0.0976 |
Weighted residual factors for all reflections included in the refinement | 0.0982 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.05 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7159588.html
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Users of the data should acknowledge the original authors of the
structural data.