New Generation of Highly Reactive Allylborating Agents For Cu(I)-Catalyzed Allylation of Chiral Sulfinylimines
Authors of publication
Alexeev, Michael S.; Strelkova, Tatyana V.; Ilyin, Jr., Michail M.; Nelyubina, Yulia V.; Bespalov, Ivan A.; Medvedev, Michael; Khrustalev, Victor N.; Kuznetsov, Nikolai
Journal of publication
Organic & Biomolecular Chemistry
Year of publication
2024
a
10.7916 ± 0.0004 Å
b
6.2242 ± 0.0002 Å
c
11.7768 ± 0.0004 Å
α
90°
β
108.897 ± 0.002°
γ
90°
Cell volume
748.4 ± 0.05 Å3
Cell temperature
100 K
Ambient diffraction temperature
100 K
Number of distinct elements
5
Space group number
4
Hermann-Mauguin space group symbol
P 1 21 1
Hall space group symbol
P 2yb
Residual factor for all reflections
0.0347
Residual factor for significantly intense reflections
0.0316
Weighted residual factors for significantly intense reflections
0.075
Weighted residual factors for all reflections included in the refinement
0.0767
Goodness-of-fit parameter for all reflections included in the refinement