Crystallography Open Database

Information card for entry 7159929

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Coordinates	7159929.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H25 N O4
Calculated formula	C24 H25 N O4
Title of publication	Highly Enantio- and Diastereoselective Construction of Spirocyclic Oxindoles via a Palladium-Catalyzed Decarboxylative Asymmetric [4 + 2] Annulation Strategy
Authors of publication	You, Pengyuan; Liu, Minjie; Zhang, Ke; Yang, Fan; Tan, Zequn; Chen, Fener
Journal of publication	Organic & Biomolecular Chemistry
Year of publication	2024
a	8.0358 ± 0.0003 Å
b	10.9125 ± 0.0004 Å
c	12.2549 ± 0.0005 Å
α	90°
β	90.715 ± 0.001°
γ	90°
Cell volume	1074.56 ± 0.07 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	4
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0305
Residual factor for significantly intense reflections	0.0295
Weighted residual factors for significantly intense reflections	0.078
Weighted residual factors for all reflections included in the refinement	0.0793
Goodness-of-fit parameter for all reflections included in the refinement	1.059
Diffraction radiation wavelength	1.34139 Å
Diffraction radiation type	GaKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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